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Chemistry Laboratory Report 1 | Trường Đại học Quốc tế, Đại học Quốc gia Thành phố HCM
Chemistry Laboratory Report 1 | Trường Đại học Quốc tế, Đại học Quốc gia Thành phố HCM được sưu tầm và soạn thảo dưới dạng file PDF để gửi tới các bạn sinh viên cùng tham khảo, ôn tập đầy đủ kiến thức, chuẩn bị cho các buổi học thật tốt. Mời bạn đọc đón xem!
Chemistry Laboratory (CH012IU) 59 tài liệu
Trường Đại học Quốc tế, Đại học Quốc gia Thành phố Hồ Chí Minh 696 tài liệu
Chemistry Laboratory Report 1 | Trường Đại học Quốc tế, Đại học Quốc gia Thành phố HCM
Chemistry Laboratory Report 1 | Trường Đại học Quốc tế, Đại học Quốc gia Thành phố HCM được sưu tầm và soạn thảo dưới dạng file PDF để gửi tới các bạn sinh viên cùng tham khảo, ôn tập đầy đủ kiến thức, chuẩn bị cho các buổi học thật tốt. Mời bạn đọc đón xem!
Môn: Chemistry Laboratory (CH012IU) 59 tài liệu
Trường: Trường Đại học Quốc tế, Đại học Quốc gia Thành phố Hồ Chí Minh 696 tài liệu
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Tài liệu khác của Trường Đại học Quốc tế, Đại học Quốc gia Thành phố Hồ Chí Minh
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CHEMISTRY LABORATORY REPORT
EXPERIMENT 1: CHEMICAL REACTIONS Group: 4 Section: 1910 Group members: Lê Nguyễn Vân Anh Hoàng Nguyễn Minh Châu Lê Thanh Như Quỳnh Trần Băng Châu Tạ Thị Minh Thu Date: February 18th, 2019. Score:
International University, Vietnam National University - HCMC 2 GENERAL CHEMISTRY LABORATORY I.Introduction:
Chemical changes result in the formation of new substances. When a chemical reaction
occurs, substances called reactants are transformed into different substances called products that
often have different appearances and different properties. Observable signs of chemical reactions
can be a change in color, the formation o f a solid, t he re lease o f g as, a nd t he p roduction o f h eat a nd
light. We also learn how to classify chemical reactions. One classification system involves five general types of reactions: s ynthesis, d
ecomposition, single displacement, double displacement, and
combustion. Chemical reaction always happens in the living system, typically the formation and transformation of matter. II.Learning Objective:
-To perform different types of chemical reactions (acid-base, precipitate, gas forming,
complex compound forming, and oxidation-reduction reactions).
-To identify some of the products in these reactions and describe the chemical changes.
-To write and balance the chemical equations for the reactions observed. III.Materials and Equipment: Equipment Test tubes Alcohol lamp Test tube rack Looped wire Test tube holders Distilled water bottle Beakers Materials Semester II: 2018-2019
International University, Vietnam National University - HCMC 3 GENERAL CHEMISTRY LABORATORY 0.5M CuSO Concentrated CH COOH 4 3 2M NaOH 0.5M Na SO 2 3 6M NaOH 0.1M KSCN 0.1M AgNO 2M KOH 3 0.5M KBr 0.5M K [Fe(CN) ] 4 6 0.5M KI 0.5M FeSO4 0.1M KI 0.5M FeCl3 2M NH OH 0.5M Al (SO ) 4 2 4 3 3% H O 2M HCl 2 2 2M H SO 0.5M LiCl 2 4 MnO 0.5M NaCl 2 Saturated FeSO 0.5M KCl 4 0.1M NaNO 0.5M CaCl 3 2 0.1M NaNO 0.5M BaCl 2 2 0.1M KMnO4 0.5M K Cr O 2 2 7 C H OH 96% H SO 2 5 2 4 2M H SO 2 4
IV. Experimental Procedure: Data and Observations: 1. Reactions of Cu2+
-First, put 10 drops of 0.5M CuSO into each of three test tubes. 4 -Then added 10 drops of 2M N aOH i nto t he fi rst test t ube; 2 M N H OH i nto t he s econd t est t ube; 4
0.5M K [Fe(CN) ] into the third one. 4 6 - A fe w s econds l ater, added more 1 0 d rops of 2 M NaOH into t he fi
rst test t ube; 2M NH OH into 4 the second test tube. Reaction Observation Chemical Equation Image 0.5M CuSO
-The blue precipitate CuSO + 2 NaOH → Cu(OH) 4 4 2 + 2M NaOH and colloidal + Na SO 2 4 phenomena were formed Semester II: 2018-2019
International University, Vietnam National University - HCMC 4 GENERAL CHEMISTRY LABORATORY Explanation:
* CuSO is dissociated completely: 4
CuSO → Cu2++ SO 2- 4 4
* NaOH is also dissociated completely to form Hydroxide ion OH-:
NaOH → Na+ + OH-
*Ion Cu2+and OH-in the solution combine together to form Cu(OH) , a blue precipitate. 2 0.5M CuSO -First, the blue
CuSO + 2NH OH → Cu(OH) + 4 4 4 2 + 2M NH OH precipitate dissolved (NH ) SO 4 4 2 4 after being formed. Then, the solution Cu(OH) + 4NH 2 → 3 turned into dark blue. [Cu(NH ) ](OH) 3 4 2 Explanation:
* CuSO is dissociated completely: 4 CuSO 2+ 2-. 4 → Cu + SO 4
* NH OH is also dissociated completely: 4
NH OH → NH4++ OH- 4
*Ion Cu2+and OH-in the solution combine together to form blue precipitate Cu(OH) because it has 2 very low solubility.
*Then, the remaining NH OH reacts with the precipitate Cu(OH) to form a 4 2
complex-compound [Cu(NH ) ]SO4 to form the dark blue of the solution. 3 4 0.5M CuSO -The
brown 2CuSO +K Fe(CN) → 4 4 4 6 0.5M K [Fe(CN) ] precipitate
and Cu [Fe(CN) ] + 2K SO 4 6 2 6 2 4 colloidal phenomena were formed. Explanation:
* Copper (II) sulfate CuSO is dissociated completely: 4
CuSO → Cu2+ + SO42- 4 Comments:
● The feature of Cu2+ is it can react with OH- form blue precipitation.
● The solution Cu(OH) also react with NH OH to form a c omplex c ompound s o reaction 2 has 2 4 the dark blue at the end.
● The last precipitate solution has brown color because the solution is compound consist of Fe2+
● Double displacement reaction occurs when part of one reactant is replaced by part of another reactant. Semester II: 2018-2019
International University, Vietnam National University - HCMC 5 GENERAL CHEMISTRY LABORATORY ● Comparing: -
The color of second precipitate is less dark than in practice. -
The color of third precipitate is just only brown unlike red-brown in practical.
2. Reactions of silver halides
-Prepared 0.5 M solutions of KCl, KBr, and KI.
-Then added 10 drops of 0.1M silver nitrate to 10 drops of each salt solution: KCl, KBr, and KI. Observing the result
-Next, we divided each of the solutions equally into two test tubes labeled # 1-3 A and # 1-3 B
*With test tube #1-3 A: did not add anything, just observe.
*With test tube # 1-3 B: added 5 drops of 2M NH OH to each of test tubes. 4
-Waited till the end of the solution and recorded the observation. Reaction Observation Chemical Equation Image 0.5M KCl
-The white precipitate AgNO + KCl → AgCl + KNO 3 3 + 0.1M AgNO was formed. 3 Explanation:
*KCl dissociate completely to form Cl-
*In the solution, ion Cl- combine with ion Ag+ to fo rm A
gCl which i s a white precipitate because they have low solubility. 0.5M KCl
-The white precipitate AgNO + KCl → AgCl + KNO 3 3 + 0.1M AgNO was formed. 3 + 2M NH OH -After adding NH OH, AgCl + 2NH OH → 4 4 4
the precipitate was [Ag(NH ) ]Cl + H O 3 2 2 dissolved slowly. Explanation:
*The precipitate AgCl reacts with Ammonium hydroxide NH OH to create the complex – compound 4
[Ag(NH ) ]Cl, which solute completely in the solution. 3 2 Semester II: 2018-2019
International University, Vietnam National University - HCMC 6 GENERAL CHEMISTRY LABORATORY 0.5M KBr -The light yellow AgNO + KBr →AgBr + KNO 3 3 + 0.1M AgNO precipitate was 3 formed. Explanation:
*KBr dissociate completely to form BRr-
*In the solution, ion Br- combine with ion Ag+
to form AgBr which is a white-yellow precipitate because they have low solubility. 0.5M KBr -The light yellow AgNO +KBr → AgBr + KNO 3 3 + 0.1M AgNO precipitate was 3 + 2M NH OH formed. AgBr + 2NH OH → 4 4
-After adding NH OH, [Ag(NH ) ]Br + H O 4 3 2 2 the precipitate was dissolved a little. Explanation:
*The precipitate AgBr reacts with NH OH to create the complex-compound [Ag(NH ) ]Br, which 4 3 2
solute completely in the solution. 0.5M KI
-The milky- white AgNO + KI → AgI + KNO 3 3 + 0.1M AgNO yellow. 3 Explanation:
*KI dissociate completely to form I-
*In the solution, ion I- combine with ion Ag+
to form AgI which is a light yellow precipitate because they have low solubility. Semester II: 2018-2019
International University, Vietnam National University - HCMC 7 GENERAL CHEMISTRY LABORATORY 0.5M KI -The milky- white
AgI+2NH OH → [Ag(NH ) ]I 4 3 2 + 0.1M AgNO3 yellow precipitate + H O 2 + 2M NH OH appeared. 4 -After adding NH OH, 4 the precipitate dissolved hardly. Explanation:
*The precipitate AgI reacts with NH OH to create a milky yellow complex – compound [Ag(NH ) ]I, 4 3 2
which solute completely in the solution. Comments:
● All those experiments prove the properties of silver halides, which is: -
Forming precipitate when reacts with salt. -
All kind of precipitate dissolved a little in NH OH liquid. 4 -
The complex compound forming and precipitation reaction are determined by this experiment. ● Comparing: -
The precipitation color of AgI, AgBr is more lightly, muddy than in practical -
The precipitation didn’t dissolve completely and fastly like in practical 3. Reactions of H O 2 2
-First, we put 5 drops of 0.1 M KMnO solution into a test tube.To continue, we added 5 drops of 4
2M H SO and then added 5 drops of 3 % H O solution into the test tube above. Finally, we 2 4 2 2
observed the change in the color and the release of gas -With a new test tube which c ontain 5 d rops of 0 .1 M K I s olution, w e c ontinued t o add 5 drops o f 2
M H SO t o acidify the KI solution a bove. Later o n, w e a dded 5 drops o f 3 % H O solution a nd had 2 4 2 2 an observation.
-In the third reaction, we added a “pinch” of solid Mn O i nto 1 mL o f 3 % H O s olution. T hen, w e 2 2 2
observed the released gas from the tube. Reaction Observation Chemical Equation Image Semester II: 2018-2019
International University, Vietnam National University - HCMC 8 GENERAL CHEMISTRY LABORATORY 0.1M KMnO
-The violet color of 2KMnO + 3H SO + 5H O → 4 4 2 4 2 2 + 2M H SO KMnO did n
ot change 8H O + 2MnSO + 5O + K SO 2 4 4 2 4 2 2 4 + H O when H SO was 2 2 2 4 added. -After adding H O , 2 2 the solution changed into transparent. The gas (as bubbles) and heat were released. Explanation:
*Due to the reducing properties of H O ; therefore, when reacting with a strong oxidizer like KMnO 2 2 4
in the acidic solution, H O is oxidized to Oxygen O which released gas as bubbles, and KMnO 2 2 2 4
loses its color. So, the solution is transparent (K SO and MnSO is non-color). 2 4 4 *In this reaction, oxygen in H O h as o xidation number -1 i s o xidized t o 0 i n O , and Mn (in K MnO ) 2 2 2 4 +7 is reduced to Mn +2. 0.1M KI
-After adding H O , 2KI + H SO + H O → K SO 2 2 2 4 2 2 2 4 + 2M H SO the transparent + 2H O + I 2 4 2 2 + H O solution quickly 2 2 changed into orange-yellow color, and a dark purple precipitate formed. Explanation:
*Because H O has oxidizing properties; therefore, when reacting with KI- a reducing agent in the 2 2
acidic solution, O-1 is reduced to O-2 in KOH, then KOH reacts with H SO to create K SO . KI is 2 4 2 4
oxidized to I , which makes the orange-yellow solution and precipitate is created. 2
*In this reaction, oxygen in H O with oxidation number -1 i s reduced t o -2 , and iodide I (in KI) -1 is 2 2 oxidized to 0 in I . 2 H O
-After adding MnO , 2H O → O + 2H O 2 2 2 2 2 2 2 + MnO the gas and heat were 2 released. The black solid did not dissolve. Semester II: 2018-2019
International University, Vietnam National University - HCMC 9 GENERAL CHEMISTRY LABORATORY Explanation: *MnO is a catalyst. 2
*H O is unstable and easy to be decomposed. When adding a “pinch” of MnO to the Hydrogen 2 2 2
peroxide (H O ) solution, H O is decomposed, with MnO as a catalyst, forming H O and releases 2 2 2 2 2 2
the gas – Oxygen (O ) (Self-redox reaction). Besides, it is also an e xothermic reaction d ue t o the heat 2 released. Comments:
● From the table above, we can see that H O has oxidizing properties also reducing properties, 2 2
and easy to be decomposed. When reacts with different substance involved, H O represents 2 2
different chemical properties of it.
● The last reaction is a self-redox reaction. This reaction also let us know that MnO is a catalyst. 2
● All reactions help us understand clearly about chemical properties of H O , the self-redox 2 2
reaction and learn more new chemical equations. 4. Reactions of Nitrate -At first, we added 1 mL o f saturated Fe SO into o ne t est t ube a nd 1 mL of 1 M NaNO s olution w as 4 3 added into another.
-Next, we poured concentrated sulfuric acid (96%) s lowly a nd c arefully d own the inside wall of t he
test tube. After a few seconds, we recorded the change of color at the interface b etween the nitrate
solution and the concentrated sulfuric acid.
-In the second stage, we replaced FeSO by NaNO . 4 3 Reaction Observation Chemical Equation Image 1M NaNO -The heat and reddish 3 2NaNO + 6FeSO + 4 + FeSO brown gas were 3 4 4 H SO → Na SO + + concentrated H SO released. 2 4 2 4 2 4 -The
transparent 2NO + 3Fe (SO ) + 2 4 3 solution changed to 4H O 2 brownish yellow. 2NO + O → 2NO 2 2
Explanation: *This is a redox reaction:
*Iron (II) sulfate (FeSO ), Sulfuric acid (H SO ) and Sodium nitrate (NaNO ) are dissociated 4 2 4 3 completely to ions:
FeSO → Fe2+ + SO 2- 4 4
H SO → 2H+ + SO 2- 2 4 4 Semester II: 2018-2019
International University, Vietnam National University - HCMC 10 GENERAL CHEMISTRY LABORATORY
NaNO → Na+ + NO - 3 3
*In the solution, with the presence o f H+, Fe 2+ is o
xidized t o Fe3+, and N w ith t he o xidation n umber + 5 in ion NO - +2
, is reduced to N in NO and NO is gas, so NO is released. 3
*The non-color gas released is NO, NO is oxidized by O , forming NO , which is reddish brown. 2 2
*After the reaction, Fe (SO ) is created and its color is b rownish y ellow w hile N a SO is t ransparent, 2 4 3 2 4
so the color of the solution after reacting depends on the color of Fe (SO ) . 2 4 3 1M NaNO -The liquid was * 2NaNO + 2FeSO + 2 2 4 + FeSO brown-black
when 3H SO → 2NaHSO 4 2 4 4 + concentrated H SO FeSO was added. + Fe (SO ) + 2NO + 2 4 4 2 4 3 -After adding 96% 2H O 2 H SO , the heat and 2 * 2NO + O → 2NO 4 2 2 reddish brown gas were released, and the color of liquid changed into brownish yellow.
Explanation: *This is also a redox reaction
*Iron (II) sulfate (FeSO ), Sulfuric acid (H SO ) and Sodium nitrite (NaNO ) are dissociated 4 2 4 2 completely to ions:
FeSO → Fe2+ + SO 2- 4 4
H SO → 2H+ + SO 2- 2 4 4
NaNO → Na+ + NO - 2 2
*In the solution, Fe2+ is oxidized to Fe3+, and N in NaNO has the oxidation number + 3, it is reduced 2
to +2 in NO (gas), then the gas is released.
*The non-color gas released is NO, NO is oxidized by O , forming NO , which is reddish brown. 2 2
*After the reaction, Fe (SO ) i s c reated a nd its color i s b rownish y ellow w hile N aHSO is t ransparent, 2 4 3 4
so the color of the solution after reacting depends on the color of Fe (SO ) . 2 4 3 1M NaNO
-The solution was split * NaNO + FeSO + 3 3 4 + FeSO
into two layers. The CH COOH → NaNO 4 3 2 +concentrated
upper was blood red, + 2(CH COO) Fe + 3 3 CH COOH
and the lower was 2SO + 3H O 3 3 2 transparent (maybe a * (CH COO) Fe + 3 3
little yellow). In the 3H O → Fe(OH) + 2 3 middle, some 3CH COOH 3 precipitate was created. Semester II: 2018-2019
International University, Vietnam National University - HCMC 11 GENERAL CHEMISTRY LABORATORY
Explanation: *This is another redox reaction.
*Iron (II) sulfate FeSO , Acetic acid CH COOH 4 3
and Sodium nitrite NaNO are dissociated completely to ions: 2
FeSO → Fe2+ + SO 2- 4 4
CH COOH → CH COO- + H+ 3 3
NaNO → Na+ + NO - 3 3
*In the solution, Fe2+ is oxidized to Fe3+, and N in NaNO has the oxidation number + 5, it is reduced 3 to +3 in NaNO . 2
*The color of the upper layer is from (CH COO) Fe. The lower one may be from transparent 3 3
solutions: CH COOH, NaNO … influenced the color of the upper layer, so it has a light color. 3 2
*The precipitate is formed because (CH COO) Fe is not stable, it decomposes in solution to Fe(OH) 3 3 3
(the reddish brown precipitate ). Comments:
● From the table above, we can see when NaNO /NaNO reacts with FeSO and concentrated 3 2 4
H SO , the observation is similar. The reason is that concentrated H SO is a strong oxidizing 2 4 2 4
agent, so it can oxidize ions to the highest oxidation number. Furthermore, the substances in
these reactions do not change concentration and necessary volume to use, thus some products are the same.
● The last reaction is redox. It shows us that (CH COO) Fe is not stable. 3 3
● All reactions help us understand clearly about redox reaction and learn more new chemical equations. 5. Reactions of KMnO4
-Prepared 3 clean test tubes and labeled # 1-3.
-In the test tube # 1: we had a combination of 10 drops of 0.5 M Na2SO3and 5 drops of 2 M H2SO4.
-In the test tube # 2: we had a combination of 10 drops of 0.5 M Na 2SO3and 5 drops of 6N NaOH.
-In the test tube # 3: we had a combination of 10 drops of 0.5 M Na2SO3and 5 drops distilled water.
-In the final step, we added 5 drops of 0.1M KMnO4 to each of the test tubes. Reaction Observation Chemical Equation Image Semester II: 2018-2019
International University, Vietnam National University - HCMC 12 GENERAL CHEMISTRY LABORATORY 0.5M Na SO -The color of KMnO
2KMnO + 3H SO + 5Na SO → 2MnSO + 2 3 4 4 2 4 2 3 4 + 2M H SO disappeared.
K SO + 3H O + 5Na SO 2 4 2 4 2 2 4 + 0.1M KMnO 4 Explanation:
* In Na SO , S has the oxidation number +4, is oxidized by the strong oxidizer Potassium 2 3
permanganate KMnO in which Mn has the oxidation number +7, to form S with the oxidation number +6 4
and Mn with the oxidation number +2 in MnSO in the acidic environment (H SO ). So the color of turns 4 2 4 into non_color 0.5M Na SO
-The solution turns 2KMnO + 2NaOH + Na SO → K MnO + 2 3 4 2 3 2 4 + 6N NaOH
into a green-brown Na MnO + Na SO + H O 2 4 2 4 2 (l) + 0.1M KMnO solution and after a 4 few seconds, it turns into a brown solution. Explanation:
* In Na SO , S has the oxidation number +4, is oxidized by the strong oxidizer Potassium 2 3
permanganate KMnO in which Mn has the oxidation number +7, to form S with the oxidation number + 6 4
and Mn with the oxidation number +6 in the basic environment. Mn +6 is in the form of Potassium
manganate K MnO and Sodium manganate Na MnO , which make the solution has the green-brown color. 2 4 2 4
After a few seconds, adding more K MnO create MnO – a brown solution. 2 4 4 0.5M Na SO -The dark
brown 2KMnO + 3Na SO + H O → 2MnO + 2 3 4 2 3 2 2 + H O precipitate appears, 3Na SO + 2KOH 2 2 4 + 0.1M KMnO and the non-color 4 solution occurs when Potassium permanganate (KMnO ) loses its 4 color. Explanation:
*In Na SO , S has the oxidation number +4, is oxidized by the strong oxidizer Potassium 2 3
permanganate (KMnO ) in which Mn has the oxidation number +7, t o fo rm S with t he o xidation number + 6 4
and Mn with the oxidation number +4 in the neutral environment.
*Mn +6 is in the form of Manganese dioxide MnO which is a dark brown precipitate. 2 Comments: Semester II: 2018-2019
International University, Vietnam National University - HCMC 13 GENERAL CHEMISTRY LABORATORY
● All three equations are redox reaction, which changes the oxidation number of 1 or more elements.
● In the second experiment, in fact when adding more K MnO that create MnO – brown 2 4 4
precipitate, but we did not add enough K MnO so the solution became the brown solution 2 4
instead of the brown precipitate.
6. Reactions of Potassium Dichromate (K Cr O ) 2 2 7
-First, we added 10 drops of 0.5M K Cr O into a test tube. 2 2 7
-Second, we added 10 drops of 6M H SO and 5 drops of C H OH was added at the end. 2 4 2 5 Reaction Observation Chemical Equation Image 2M K Cr O
-When we put H SO 2K Cr O + 3C H OH + 8H SO 2 2 7 2 4 2 2 7 2 5 2 4 + 6M H SO
into K Cr O , the → 3CH COOH + 2Cr (SO ) + 2 4 2 2 7 3 2 4 3 + C H OH
color of the solution 2K SO + 11H O 2 5 2 4 2 is orange. -After we added C H OH to the test 2 5 tube, the color of the solution is dark green.
Comments: In C H OH, C has the oxidation number -1, is oxidized by the strong oxidizer 2 5
Potassium dichromate K Cr O – in which Cr has the oxidation number +6, to form C with the 2 2 7
oxidation number +1 and Cr with the oxidation number +3. The dark green color of the solution
comes from the color of the salt Cr3+ Cr (SO ) . 2 4 3 7. A. Reactions of Fe3+
-In the first step, we added 1 mL of 0.5M FeCl solution in each of the four test tubes. 3 Semester II: 2018-2019
International University, Vietnam National University - HCMC 14 GENERAL CHEMISTRY LABORATORY
-Later 5 drops of the following four reagents: 0.1M KSCN; 2M KOH;
0.5M K [Fe(CN) ]; 2M NH OH was added to four test tubes which contained FeCl solution in turn. 4 6 4 3
-At the end of the reaction, we had observations Reaction Observation Chemical Equation Image 0.5M FeCl -The solution c
hanged FeCl + 3KSCN→ K [Fe(SCN) ] + 3 3 3 6 + 0.1M KSCN the color into blood 3KCl color (red-brown color). Explanation:
FeCl reacts with potassium thiocyanate (KSCN) to form the complex compound K [Fe(SCN) ], 3 3 6
which is a red-brown solution. 0.5M FeCl -A brownish
red FeCl + 3KOH → Fe(OH) + 3KCl 3 3 3 + 2M KOH precipitate was formed. Explanation:
*FeCl and KOH dissociate in the solution to create ions Fe3+and OH-, then these two ions combine 3
together to form brownish-red precipitate Fe(OH) . 3
FeCl → Fe3+ + 3Cl- 3 KOH → K+ + OH- ⇒ F
e3+ + 3OH-→ Fe(OH) ↓ 3 0.5M FeCl -Forming a dark blue 2FeCl + 3K [Fe(CN) ] → 3 3 4 6
+ 0.5M K [Fe(CN) ] precipitate. Fe [Fe(CN) ] + 12KCl 4 6 4 6 3 Explanation:
FeCl reacts with potassium ferrocyanide (K [Fe(CN) ]) to form a complex compound Iron(III) 3 4 6
ferrocyanide (Fe [Fe(CN) ] ), which is dark blue precipitate. 4 6 3 Semester II: 2018-2019
International University, Vietnam National University - HCMC 15 GENERAL CHEMISTRY LABORATORY 0.5M FeCl -The orange
FeCl + 3NH OH → Fe(OH) + 3 3 4 3 + 2M NH OH precipitate appeared. 3NH Cl 4 4 Explanation:
*FeCl and NH OH dissociate i n the solution t o create ions Fe3+ and OH-, then these t wo i ons combine 3 4
together to form a light brownish red precipitate.
FeCl → Fe3+ + 3Cl- 3
NH OH → NH + + OH - 4 4 ⇒ F
e3+ + 3OH- → Fe(OH) ↓ 3 Comments:
● In fact, Fe(OH) has a brownish red color. But experiment 5 has different color precipitate. In 3
experiment 5, it creates light brownish red color because of NH OH 4 is a weak base.
● Furthermore, we can learn mo
re about the new chemical equations. 7. B. Reactions of Fe2+
-In the second stage, we did the same as what we had done before but FeSO was used instead of 4 FeCl . 3 Reaction Observation Chemical Equation Image 0.5M FeSO
-The solution changed FeSO + 2KSCN → K [Fe(SCN) ] 4 4 4 6 + 0.1M KSCN color into red-brown. + K SO 2 4 Explanation:
FeSO reacts with potassium thiocyanate K SCN t o fo
rm the complex compound K [Fe(SCN) ], w hich 4 4 6 is a red brown solution. 0.5M FeSO -A dark green
FeSO + 2KOH → Fe(OH) + 4 4 2 + 2M KOH precipitate appeared. K SO 2 4 Semester II: 2018-2019